鑱氳嫰鑳猴紙PANI錛夋槸鏈鏈夊惛寮曞姏鐨勮禎鐢靛鏉愭枡涔嬩竴銆備負浜嗗寮虹數瑙ｈ川鎵╂暎騫舵敼鍠勭數鏋佺殑鐢靛寲瀛︽ц兘錛岄渶瑕佺簿蹇冭璁＄殑PANI褰㈡併傛幒鍏ョ⒊鏉愭枡涔熸湁鍒╀簬鎻愰珮PANI鐨勫驚鐜ǔ瀹氭с佹満姊板拰鐢靛寲瀛︽ц川銆傚湪璇ョ爺絀朵腑錛屽簲鐢ㄧ畝鍗曠殑婧舵恫娉曟潵鍚堟垚棰楃矑娌夌Н鐨勭鐘禤ANI銆傜敱浜庣粨鏋勬竻鏅幫紝鍦ㄧ數嫻佸瘑搴︿負4 A/g鏃訛紝姣斿閲忥紙CF錛夎揪鍒?37.8 F/g銆傛澶栵紝灝嗚嚜鍚堟垚鐨勬哀鍖栫煶澧ㄧ儻錛圙O錛夌畝鍗曞湴涓庨綺掓矇縐殑綆＄姸PANI娣峰悎錛屼互鍒跺鏇存湁鏁堢殑鐢靛鎬ф潗鏂欍傜敱浜庢潵鑷狿ANI鐨勮禎鐢靛鍜孏O鐨勫畼鑳藉洟浠ュ強鏉ヨ嚜GO鐨勭數鍖栧鍙屽眰鐢靛鐨勫崗鍚屾晥搴旓紝浼樺寲鐨凱ANI/GO鐢墊瀬瀹炵幇浜?75.0 F/g澧炲己鐨凜F鍊箋傚湪榪涜2000嬈″驚鐜噸澶嶅厖鐢?鏀劇數榪囩▼鍚庯紝瀵逛簬浼樺寲鐨凱ANI/GO鐢墊瀬錛屼篃鑾峰緱90錛呯殑CF淇濈暀鐜囧拰楂樹簬90錛呯殑騫沖潎搴撲粦鏁堢巼銆?/span>
Fig. 1. 浣跨敤錛坅錛?銆侊紙b錛?2銆侊紙c錛?8銆侊紙d錛?4鍜岋紙e錛?6 h鍒跺鐨凷EM鍥撅紱浣跨敤24灝忔椂鍒跺PANI鐨勶紙f錛塗EM鍥懼拰錛坓錛塃DX鍏夎氨鍥俱?/span>
Fig. 2. 澶嶅悎鏉愭枡鐨凷EM鍥撅紝PANI:GO姣旂巼涓猴紙a錛?:1銆侊紙b錛?:2銆侊紙c錛?:1銆侊紙d錛?:1鍜岋紙e錛?:0銆?/span>
Fig. 3. 錛坅錛変互10 mV/s鑾峰緱鐨凜V鏇茬嚎鍜岋紙b錛変嬌鐢ㄤ笉鍚屾椂闂村埗澶囩殑PANI鐢墊瀬錛屼互4 A/g鑾峰緱鐨凣C/D鏇茬嚎錛涗嬌鐢?4灝忔椂鍒跺鐨凱ANI鐢墊瀬錛岋紙c錛夊湪鍚勭鎵弿閫熺巼涓嬫祴閲忕殑CV鏇茬嚎鍜岋紙d錛夊湪涓嶅悓鐢墊祦瀵嗗害涓嬫祴閲忕殑GC/D鏇茬嚎銆?/span>
Fig. 4. PANI銆丟O鍜屼笉鍚孭ANI涓嶨O姣旂巼鐨凱ANI/GO鐢墊瀬錛岋紙a錛変互10 mV/s鎵弿閫熺巼嫻嬮噺鐨凜V鏇茬嚎鍜岋紙b錛夊湪5 A/g鐨勭數嫻佸瘑搴︿笅嫻嬮噺鐨凣C/D鏇茬嚎錛涗笉鍚孭ANI鍜孏O姣旂巼鐨凱ANI/GO鐢墊瀬鐨勶紙c錛夊濂庢柉鐗瑰浘鍜岋紙d錛夌浉搴旂瓑鏁堢數璺紱PANI涓嶨O鐨勬瘮渚嬩負1錛?錛屼紭鍖栫殑PANI/GO鐢墊瀬錛岋紙e錛変笉鍚屾壂鎻忛熺巼嫻嬮噺鐨凜V鏇茬嚎銆侊紙f錛変笉鍚岀數嫻佸瘑搴︽祴閲忕殑GC/D鏇茬嚎銆侊紙g錛変粠CV鏇茬嚎鑾峰緱CF鍊間笌鐩稿簲鎵弿閫熺巼涔嬮棿鐨勫叧緋誨浘浠ュ強錛坔錛変粠GC/D鏇茬嚎鑾峰緱CF鍊煎拰鐩稿簲鐢墊祦瀵嗗害涔嬮棿鐨勫叧緋誨浘銆?
鐩稿叧鐮旂┒鎴愭灉浜?018騫寸敱鍙板寳縐戞妧澶уLu-Yin Lin璇鵑緇勶紝鍙戣〃鍦‥lectrochimica Acta錛坔ttps://doi.org/10.1016/j.electacta.2017.10.195錛変笂銆傚師鏂囷細Enhanced electrocapacitive performance for the supercapacitor with tube-like polyaniline and graphene oxide composites錛圗lectrochimica Acta 259 (2018) 348e354錛夈?
