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澶嶅悎鏉愭枡
褰撳墠浣嶇疆錛?棣栭〉 >> 璧勮 >> 澶嶅悎鏉愭枡 >> 琛屼笟鍔ㄦ?/a> >> 姝ｆ枃

姘?/span>鎬?/span>鍙?/span>鍏?/span>鐢?/span>閿?/span>紱?/span>瀛?/span>鐢?/span>姹?/span>錛?/span>ZIBs錛?/span>鍥?/span>鍏?/span>瀹?/span>鍏?/span>鎬?/span>楂?/span>銆?/span>瀹?/span>閲?/span>澶?/span>錛?/span>鐞?/span>璁?/span>瀹?/span>閲?/span>涓?/span>820 mah/g錛?/span>鑰?/span>寮?/span>璧?/span>浜?/span>浜?/span>浠?/span>鐨?/span>鏋?/span>澶?/span>鍏?/span>瓚?/span>閿?/span>鐨?/span>楂?/span>涓?/span>搴?/span>銆?/span>浣?/span>鎴?/span>鏈?/span>鍜?/span>浣?/span>姘?/span>鍖?/span>榪?/span>鍘?/span>鐢?/span>浣?/span>(涓?/span>鏍?/span>鍑?/span>姘?/span>鐢?/span>鏋?/span>鐩?/span>姣?/span>涓?/span>0.76 V錛?/span>銆?/span>鐩?/span>鍓?/span>錛?/span>ZIBs鐨?/span>涓?/span>瑕?/span>闅?/span>紕?/span>涔?/span>涓鏄?/span>闃?/span>鏋?/span>鏉?/span>鏂?/span>鐨?/span>鏈?/span>闄?/span>閫?/span>鎷?/span>銆?/span>Zn2 鐨?/span>楂?/span>鏋?/span>鎬?/span>浣?/span>寰?/span>涓?/span>闃?/span>鏋?/span>涓?/span>浣?/span>鐨?/span>闈?/span>鐢?/span>鐩?/span>浜?/span>浣?/span>鐢?/span>姣?/span>Li 絳?/span>涓浠?/span>闃?/span>紱?/span>瀛?/span>鏇?/span>寮?/span>錛?/span>瀵?/span>鑷?/span>鎵?/span>鏁?/span>鍔?/span>鍔?/span>瀛?/span>鎱?/span>寰?/span>澶?/span>錛?/span>婧?/span>瑙?/span>搴?/span>浣?/span>銆?/span>姝?/span>澶?/span>錛?/span>鐢?/span>鏋?/span>鏉?/span>鏂?/span>鐨?/span>鏋?/span>姘?/span>鐢?/span>浣?/span>銆?/span>姘?/span>鍖?/span>榪?/span>鍘?/span>鐢?/span>浣?/span>鍙?/span>鍏?/span>緇?/span>鏋?/span>紼?/span>瀹?/span>鎬?/span>涔?/span>闄?/span>鍒?/span>浜?/span>鍏?/span>鍦?/span>姘?/span>鐢?/span>瑙?/span>娑?/span>涓?/span>鐨?/span>宸?/span>浣?/span>鐢?/span>鍘?/span>銆?/span>


榪?/span>鏈?/span>錛?/span>瀹?/span>寰?/span>鐞?/span>宸?/span>澶?/span>瀛?/span>鍖?/span>瀛?/span>宸?/span>紼?/span>瀛?/span>闄?/span>灝?/span>鎴?/span>鏉?/span>鍗?/span>澹?/span>涓?/span>鏉?/span>鏂?/span>瀛?/span>闄?/span>娼?/span>鎴?/span>宀?/span>鏁?/span>鎺?/span>鍦?/span>閲?/span>灞?/span>鏈?/span>鏈?/span>妗?/span>鏋?/span>鏉?/span>鏂?/span>錛?/span>MOF錛?/span>姘?/span>緋?/span>閿?/span>紱?/span>瀛?/span>鍌?/span>瀛?/span>鏂?/span>闈?/span>鍙?/span>寰?/span>鏂?/span>榪?/span>灞?/span>錛?/span>涓?/span>鎻?/span>楂?/span>閲?/span>灞?/span>鏈?/span>鏈?/span>妗?/span>鏋?/span>鏉?/span>鏂?/span>鐨?/span>鐢?/span>鍖?/span>瀛?/span>鍌?/span>閿?/span>媧?/span>鎬?/span>錛?/span>璇?/span>璇?/span>棰?/span>緇?/span>璁?/span>璁?/span>鍒?/span>澶?/span>浜?/span>涓縐?/span>閰?/span>浣?/span>涓?/span>楗?/span>鍜?/span>閲?/span>灞?/span>鏈?/span>鏈?/span>妗?/span>鏋?/span>姘?/span>緋?/span>閿?/span>紱?/span>瀛?/span>姝?/span>鏋?/span>鏉?/span>鏂?/span>錛?/span>鐩?/span>鍏?/span>鎴?/span>鏋?/span>浠?/span>鏍?/span>棰?/span>涓?/span>鈥?/span>Coordinately Unsaturated Manganese-Based Metal鈥?/span>Organic Frameworks as a High-Performance Cathode for Aqueous Zinc-Ion Batteries鈥?/span>鍙?/span>琛?/span>鍦?/span>ACS Applied Materials & Interfaces銆?/span>瀹?/span>寰?/span>鐞?/span>宸?/span>澶?/span>瀛?/span>鍖?/span>瀛?/span>宸?/span>紼?/span>瀛?/span>闄?/span>灝?/span>鎴?/span>鏉?/span>鍗?/span>澹?/span>涓?/span>璁?/span>鏂?/span>絎?/span>涓浣?/span>鑰?/span>鍏?/span>閫?/span>璁?/span>銆?/span>閿?/span>鐨?/span>閰?/span>浣?/span>涓?/span>楗?/span>鍜?/span>鏄?/span>鐢?/span>涓?/span>涓?/span>鐩?/span>閭?/span>-COO-鐨?/span>姘?/span>鍘?/span>瀛?/span>榪?/span>琛?/span>鐨?/span>銆?/span>鍏?/span>閫?/span>褰?/span>鐨?/span>涓?/span>楗?/span>鍜?/span>閰?/span>浣?/span>搴?/span>淇?/span>璇?/span>浜?/span>楂?/span>鏁?/span>鐨?/span>Zn2 浼?/span>杈?/span>鍜?/span>鐢?/span>瀛?/span>浜?/span>鎹?/span>錛?/span>浠?/span>鑰?/span>淇?/span>璇?/span>浜?/span>閲?/span>澶?/span>鍏?/span>鏀?/span>鐢?/span>榪?/span>紼?/span>涓?/span>鐨?/span>楂?/span>鏈?/span>寰?/span>媧?/span>鎬?/span>鍜?/span>蹇?/span>閫?/span>鐢?/span>鍖?/span>瀛?/span>鍙?/span>搴?/span>鍔?/span>鍔?/span>瀛?/span>銆?/span>鍥?/span>姝?/span>錛?/span>鐢?/span>浜?/span>涓?/span>榪?/span>浼?/span>鐐?/span>錛?/span>榪?/span>縐?/span>鍩?/span>浜?/span>MOF鐨?/span>鐢?/span>鏋?/span>鍏?/span>鏈?/span>楂?/span>瀹?/span>閲?/span>(鍦?/span>100 mA g-1鏃?/span>涓?/span>138 mAh g-1)鍜?/span>闀?/span>瀵?/span>鍛?/span>(鍦?/span>3000 mA g-1涓?/span>寰?/span>鐜?/span>1000嬈?/span>鍚?/span>瀹?/span>閲?/span>淇?/span>鎸?/span>鐜?/span>涓?/span>93.5%)銆?/span>榪?/span>縐?/span>鐙?/span>鐗?/span>鐨?/span>Zn2 紱?/span>瀛?/span>瀛?/span>鍌?/span>鎬?/span>鑳?/span>瓚?/span>榪?/span>浜?/span>澶?/span>澶?/span>鏁?/span>鏈榪?/span>鎶?/span>閬?/span>鐨?/span>MOF闃?/span>鏋?/span>銆?/span>榪?/span>縐?/span>閫?/span>榪?/span>璋?/span>鑺?/span>閰?/span>浣?/span>搴?/span>鏉?/span>璋?/span>鑺?/span>鍌?/span>鑳?/span>鑳?/span>鍔?/span>鐨?/span>姒?/span>蹇?/span>涓?/span>鎺?/span>绱?/span>姘?/span>緋?/span>ZIBs鐨?/span>楂?/span>鎬?/span>鑳?/span>MOF闃?/span>鏋?/span>鎻?/span>渚?/span>浜?/span>鏂?/span>鐨?/span>閫?/span>寰?/span>銆?/span>姝?/span>鐮?/span>絀?/span>寰?/span>鍒?/span>瀹?/span>寰?/span>鐪?/span>閲?/span>鐐?/span>鐮?/span>鍙?/span>璁?/span>鍒?/span>絳?/span>璧?/span>鍔?/span>鏀?/span>鎸?/span>銆?/span>



鍥?/span>1. (a) Mn-H3BTC-MOF-4涓?/span>Mn(II)鐨?/span>鍚?/span>鎴?/span>榪?/span>紼?/span>鍜?/span>閰?/span>浣?/span>鐜?/span>澧?/span>紺?/span>鎰?/span>鍥?/span>銆?/span>SEM鍥?/span>鍍?/span>錛?/span>(b,e) Mn-H3BTC-MOF-2錛?/span>(c,f) Mn-H3BTC-MOF-4鍜?/span> (d,g) Mn-H3BTC-MOF-6銆?/span>



鍥?/span>2. MOFs綺?/span>鏈?/span>涓?/span>C銆?/span>O鍜?/span>Mn鍏?/span>绱?/span>鐨?/span>HRTEM鍥?/span>鍍?/span>鍜?/span>EDS鍏?/span>绱?/span>鏄?/span>灝?/span>錛?/span>(a) Mn-H3BTC-MOF-2錛?/span>(b) Mn-H3BTC-MOF-4鍜?/span> (c) Mn- H3BTC-MOF-6銆?/span>



鍥?/span>3. Mn-H3BTC-MOF-2銆?/span>Mn-H3BTC-MOF-4鍜?/span>Mn-H3BTC-MOF-6鐨?/span> (a-c) XRD璋?/span>鍥?/span>鍜?/span> (d-f) TGA-DTG璋?/span>銆?/span>



鍥?/span>4. 鍚?/span>鎴?/span>鏍?/span>鍝?/span>鐨?/span>FTIR鍏?/span>璋?/span>錛?/span>(a) Mn-H3BTC-MOF-2錛?/span>(b) Mn-H3BTC-MOF-4錛?/span>(c) Mn-H3BTC-MOF-6鍜?/span> (d) H3BTC錛?/span>浠?/span>鍙?/span>Mn-H3BTC-MOF-4鐨?/span>楂?/span>鍒?/span>杈?/span>鐜?/span> (e) 嫻?/span>閲?/span>銆?/span>(f) Mn 2p銆?/span>(g) O 1s鍜?/span> (h) C 1s XPS鍏?/span>璋?/span>銆?/span>



鍥?/span>5. (a) 鍏?/span>鏈?/span>2 M Zn(CF3SO3)2姘?/span>緋?/span>鐢?/span>瑙?/span>璐?/span>鐨?/span>MOF闃?/span>鏋?/span>鈭?/span>Zn闃?/span>鏋?/span>ZIBs鐨?/span>紺?/span>鎰?/span>鍥?/span>錛?/span>(b,c) 涓?/span>涓?/span>鏍?/span>鍝?/span>鍦?/span> 0.1 mV s?1涓?/span>鐨?/span>CV鏇?/span>綰?/span>鍜?/span>鍦?/span>100 mA g?1涓?/span>鐨?/span>鍏?/span>鏀?/span>鐢?/span> 錛?/span>(d) Mn-H3BTC-MOF-4鍦?/span>涓?/span>鍚?/span>鐢?/span>嫻?/span>瀵?/span>搴?/span>涓?/span>鐨?/span>鍏?/span>鏀?/span>鐢?/span>鏇?/span>綰?/span>錛?/span>(e) Mn-H3BTC-MOF-4(浠?/span>100鍒?/span>3000 mA g?1)鐨?/span>鍊?/span>鐜?/span>鎬?/span>鑳?/span>錛?/span>浠?/span>鍙?/span> (f,g) Mn-H3BTC-MOF-4鍒?/span>鍒?/span>鍦?/span>100鍜?/span>3000 mA g?1涓?/span>鐨?/span>寰?/span>鐜?/span>鎬?/span>鑳?/span>銆?/span>



鍥?/span>6. (a,b) 寰?/span>鐜?/span>Mn-H3BTC-MOF-4鐢?/span>鏋?/span>鍦?/span>100嬈?/span>寰?/span>鐜?/span>鍚?/span>鐨?/span>SEM鍥?/span>鍍?/span>鍜?/span>Zn鍏?/span>绱?/span>鏄?/span>灝?/span>錛?/span>(c) XRD鍥?/span>璋?/span>鍜?/span> (d) Mn 2p 錛?/span>(e) C 1s鍜?/span> (f) O 1s XPS鍏?/span>璋?/span>銆?/span>



鍥?/span>7. 涓?/span>鍚?/span>鍏?/span>鏀?/span>鐢?/span>闃?/span>孌?/span>寰?/span>鐜?/span>鐢?/span>鏋?/span>鐨?/span>闈?/span>鍘?/span>浣?/span>XRD鍥?/span>璋?/span>銆?/span>


鍥?/span>8. (a) Mn-H3BTC-MOF-4鍦?/span>涓?/span>鍚?/span>鎵?/span>鎻?/span>閫?/span>鐜?/span>涓?/span>鐨?/span>CV鏇?/span>綰?/span>錛?/span>(b) CV鏇?/span>綰?/span>涓?/span>闃?/span>鏋?/span>宄?/span>鍜?/span>闃?/span>鏋?/span>宄?/span>鐨?/span>log(宄?/span>鍊?/span>鐢?/span>嫻?/span>)涓?/span>log(鎵?/span>鎻?/span>閫?/span>鐜?/span>)鐨?/span>鍏?/span>緋?/span>鍥?/span>錛?/span>(c) 0.1 mV s?1鏃?/span>鐨?/span>鐢?/span>瀹?/span>璐?/span>鐚?/span>(姍?/span>鑹?/span>閮?/span>鍒?/span>)鍜?/span>鎵?/span>鏁?/span>璐?/span>鐚?/span>(绱?/span>鑹?/span>閮?/span>鍒?/span>)錛?/span>浠?/span>鍙?/span> (d) 涓?/span>鍚?/span>鎵?/span>鎻?/span>閫?/span>鐜?/span>涓?/span>鐢?/span>瀹?/span>姣?/span>璐?/span>鐚?/span>鐨?/span>鏌?/span>鐘?/span>鍥?/span>銆?/span>


鎬?/span>涔?/span>錛?/span>鏈?/span>鏂?/span>棣?/span>鍏?/span>鎻?/span>鍑?/span>浜?/span>涓縐?/span>鍗?/span>璋?/span>涓?/span>楗?/span>鍜?/span>絳?/span>鐣?/span>鏉?/span>澧?/span>寮?/span>ZIBs鐨?/span>Mn-H3BTC-MOF-4闃?/span>鏋?/span>鐨?/span>鍊?/span>鐜?/span>鍜?/span>寰?/span>鐜?/span>鎬?/span>鑳?/span>銆?/span>涓?/span>Mn-H3BTC-MOF-2鍜?/span>Mn-H3BTC-MOF-6鐩?/span>姣?/span>錛?/span>璇?/span>鐢?/span>鏋?/span>閫?/span>褰?/span>鐨?/span>涓?/span>楗?/span>鍜?/span>閰?/span>浣?/span>搴?/span>涓?/span>Zn2 紱?/span>瀛?/span>浼?/span>杈?/span>鎻?/span>渚?/span>浜?/span>鏇?/span>灝?/span>鐨?/span>絀?/span>闂?/span>浣?/span>闃?/span>鍜?/span>鏇?/span>浣?/span>鐨?/span>鐢?/span>瀛?/span>浼?/span>杈?/span>闃?/span>鍔?/span>銆?/span>鍥?/span>姝?/span>錛?/span>澧?/span>寮?/span>鐨?/span>璐?/span>閲?/span>鍜?/span>鐢?/span>鑽?/span>浼?/span>杈?/span>鐗?/span>鎬?/span>浠?/span>鍙?/span>瀵?/span>閿?/span>紱?/span>瀛?/span>瀛?/span>鍌?/span>鐨?/span>閫?/span>搴?/span>浜?/span>鍜?/span>鍔?/span>瀵?/span>鑷?/span>鏄?/span>钁?/span>澧?/span>寮?/span>鐨?/span>鏈?/span>寰?/span>媧?/span>鎬?/span>鍜?/span>鐢?/span>鍖?/span>瀛?/span>鍔?/span>鍔?/span>瀛?/span>銆?/span>鏈?/span>鐞?/span>鐮?/span>絀?/span>琛?/span>鏄?/span>錛?/span>Mn-H3BTC-MOF-4鐨?/span>閿?/span>鍌?/span>瀛?/span>鍙?/span>鍒?/span>涓?/span>涓?/span>涓?/span>姝?/span>楠?/span>錛?/span>(i) MOFs涓?/span>鐨?/span>Mn2 琚?/span>Zn2 緗?/span>鎹?/span>鍜?/span> (ii) Mn2 姘?/span>鍖?/span>涓?/span> MnO2騫?/span>褰?/span>鎴?/span>ZnMn3O7·3H2O鍖?/span>鍚?/span>鐗?/span>銆?/span>榪?/span>縐?/span>鍩?/span>浜?/span>MOF鐨?/span>鐢?/span>鏋?/span>鍦?/span>100 mA g?1涓?/span>鍏?/span>鏈?/span>138 mAh g?1鐨?/span>浼?/span>寮?/span>瀹?/span>閲?/span>錛?/span>騫?/span>涓?/span>鍦?/span>3000 mA g?1涓?/span>寰?/span>鐜?/span>1500嬈?/span>鍚?/span>鍏?/span>鏈?/span>93.5%鐨?/span>瓚?/span>楂?/span>瀹?/span>閲?/span>淇?/span>鎸?/span>鐜?/span>銆?/span>鎬?/span>鐨?/span>鏉?/span>璇?/span>錛?/span>Mn-H3BTC-MOF-4鐨?/span>Zn2 紱?/span>瀛?/span>瀛?/span>鍌?/span>鎬?/span>鑳?/span>瓚?/span>榪?/span>浜?/span>鏈榪?/span>鎶?/span>閬?/span>鐨?/span>澶?/span>澶?/span>鏁?/span>MOF闃?/span>鏋?/span>銆?/span>榪?/span>欏?/span>宸?/span>浣?/span>涓?/span>鎺?/span>绱?/span>鍗?/span>璋?/span>涓?/span>楗?/span>鍜?/span>MOF鏉?/span>鏂?/span>浠?/span>瀹?/span>鐜?/span>楂?/span>鎬?/span>鑳?/span>ZIBs鎻?/span>渚?/span>浜?/span>鏂?/span>閫?/span>寰?/span>銆?/span>


鐩?/strong>鍏?/strong>閾?/strong>鎺?/strong>

Chengjie Yin*, Chengling Pan*, Xiaobo Liao, Yusong Pan*, and Liang Yuan*. Coordinately Unsaturated Manganese-Based Metal鈥?/span>Organic Frameworks as a High-Performance Cathode for Aqueous Zinc-Ion Batteries. ACS Appl. Mater. Interfaces

https://doi.org/10.1021/acsami.1c10063

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